5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

Base Information

Chemical Name:5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol
CAS No.:959838-30-3
Molecular Formula:C₃₁H₂₅BrN₄O₃
Molecular Weight:581.468
Hs Code.:

Synonyms:5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

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Chemical Property of 5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

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Technology Process of 5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

There total 7 articles about 5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174007-94-3
N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

: 959838-30-3
5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

Guidance literature:: With sodium hydroxide; potassium hexacyanoferrate(III); In ethanol; Heating / reflux;

Reference yield:

: 912545-14-3
benzyl 2,4-bis(benzyloxy)-5-bromobenzoate

: 959838-30-3
5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol; sodium hydroxide; water / Heating / reflux

1.2: pH 2

2.1: lithium aluminium tetrahydride / tetrahydrofuran

3.1: manganese(IV) oxide / dichloromethane / 72 h / Heating / reflux

4.1: ethanol / 1 h / Heating / reflux

5.1: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol / Heating / reflux

With methanol; manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; water; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 898538-48-2
2,4-bis-benzyloxy-5-bromo-benzyl alcohol

: 959838-30-3
5-(2,4-bis-benzyloxy-5-bromo-phenyl)-4-(1-methyl-1H-indol-5-yl)-4H-[1,2,4]triazol-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: manganese(IV) oxide / dichloromethane / 72 h / Heating / reflux

2: ethanol / 1 h / Heating / reflux

3: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol / Heating / reflux

With manganese(IV) oxide; sodium hydroxide; potassium hexacyanoferrate(III); In ethanol; dichloromethane;