N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

Base Information

Chemical Name:N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide
CAS No.:1174007-94-3
Molecular Formula:C₃₁H₂₇BrN₄O₃
Molecular Weight:583.484
Hs Code.:

Synonyms:N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

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Chemical Property of N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

Chemical Property:

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Technology Process of N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

There total 6 articles about N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 898538-49-3
2,4-bis-benzyloxy-5-bromo-benzaldehyde

: 958888-24-9
N-(1-methyl-1H-indol-5-yl)hydrazinecarboxamide

: 1174007-94-3
N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

Guidance literature:: In ethanol; for 1h; Heating / reflux;

Reference yield:

: 912545-10-9
2,4-bis(benzyloxy)-5-bromobenzoic acid

: 1174007-94-3
N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran

2: manganese(IV) oxide / dichloromethane / 72 h / Heating / reflux

3: ethanol / 1 h / Heating / reflux

With manganese(IV) oxide; lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 912545-14-3
benzyl 2,4-bis(benzyloxy)-5-bromobenzoate

: 1174007-94-3
N-(1-methyl-1H-indol-5-yl)-N''-(2,4-bis-benzyloxy-5-bromo-benzylidene)-semicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; sodium hydroxide; water / Heating / reflux

1.2: pH 2

2.1: lithium aluminium tetrahydride / tetrahydrofuran

3.1: manganese(IV) oxide / dichloromethane / 72 h / Heating / reflux

4.1: ethanol / 1 h / Heating / reflux

With methanol; manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; water; In tetrahydrofuran; ethanol; dichloromethane;