Phenylmethyl 1,1,1-trichloromethanesulfenate

Base Information

Chemical Name:Phenylmethyl 1,1,1-trichloromethanesulfenate
CAS No.:13029-10-2
Molecular Formula:C₈H₇Cl₃OS
Molecular Weight:257.568
Hs Code.:
DSSTox Substance ID:DTXSID601255458

Synonyms:Phenylmethyl 1,1,1-trichloromethanesulfenate;DTXSID601255458;13029-10-2

Suppliers and Price of Phenylmethyl 1,1,1-trichloromethanesulfenate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenylmethyl 1,1,1-trichloromethanesulfenate

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:255.928319
Heavy Atom Count:13
Complexity:143

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COSC(Cl)(Cl)Cl

Technology Process of Phenylmethyl 1,1,1-trichloromethanesulfenate

There total 1 articles about Phenylmethyl 1,1,1-trichloromethanesulfenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 594-42-3
chlorothio-trichloro-methane

: 100-51-6,185532-71-2
benzyl alcohol

: 13029-10-2
Benzyl trichloromethanesulfenate

Guidance literature:: With pyridine;
DOI:10.1016/S0040-4020(01)97107-8

Reference yield: 98.0%

: 13029-10-2
Benzyl trichloromethanesulfenate

: 55613-64-4
Benzyl trichloromethanesulfinate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 0 deg C, 2.) 1 h, room temperature;
DOI:10.1016/S0040-4020(01)88389-7

Reference yield:

: 13029-10-2
Benzyl trichloromethanesulfenate

: 15894-11-8
Benzyl trichloromethyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 80percent MCPBA / CH₂Cl₂ / 1.) 0 deg C, 2.) 1 h, room temperature

2: 75 percent / 2,6-lutidine / acetonitrile / 4.5 h / 100 °C

With 2,6-dimethylpyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)88389-7