Technology Process of C14H20O2
There total 4 articles about C14H20O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
diethyl ether; water; acetonitrile;
at 20 ℃;
DOI:10.1039/c6ob00347h
- Guidance literature:
-
1-bromo-4-tert-butylbenzene;
With
tert.-butyl lithium;
In
diethyl ether; pentane;
at -78 ℃;
for 1h;
4-butanolide;
In
diethyl ether; pentane;
at -78 ℃;
for 1h;
DOI:10.1002/anie.201409572
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol
2: potassium tert-butylate / tetrahydrofuran; ethanol / 4 h / 20 °C
3: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate / acetonitrile; water; diethyl ether / 20 °C
With
sodium tetrahydroborate; potassium tert-butylate; 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water; acetonitrile;
DOI:10.1039/c6ob00347h