(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

Base Information

Chemical Name:(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate
CAS No.:1450591-23-7
Molecular Formula:C₂₉H₃₃NO₆
Molecular Weight:491.584
Hs Code.:

Synonyms:(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

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Chemical Property of (E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

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Technology Process of (E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

There total 5 articles about (E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

: 1200-03-9
4-bromophenyl butyl ether

: 1450590-86-9
(E)-ethyl 3-{5-{[2-(benzo[d][1,3]dioxol-5-yl)ethylamino]methyl}furan-2-yl}acrylate

: 1450591-23-7
(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 35 ℃; for 8h;
DOI:10.1016/j.bmc.2013.06.009

Reference yield:

: 53282-12-5,53282-26-1
ethyl (E)-3-(2-furyl)prop-2-enoate

: 1450591-23-7
(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate; N,N-dimethyl-formamide / 2.33 h / 0 - 60 °C

2: methanol / 3 h / Reflux

3: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

4: potassium iodide; potassium carbonate / acetonitrile / 8 h / 35 °C

With sodium tetrahydroborate; potassium carbonate; N,N-dimethyl-formamide; potassium iodide; trichlorophosphate; In methanol; acetonitrile;
DOI:10.1016/j.bmc.2013.06.009

Reference yield:

: 191480-39-4
ethyl (E)-3-(5-formylfuran-2-yl)acrylate

: 1450591-23-7
(E)-ethyl 3-{5-{{[2-(benzo[d][1,3]dioxol-5-yl)ethyl](2-phenoxybutyl)amino}methyl}furan-2-yl}acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

3: potassium iodide; potassium carbonate / acetonitrile / 8 h / 35 °C

With sodium tetrahydroborate; potassium carbonate; potassium iodide; In methanol; acetonitrile;
DOI:10.1016/j.bmc.2013.06.009