3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

Base Information

Chemical Name:3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene
CAS No.:108634-78-2
Molecular Formula:C₂₁H₃₁NO₄Si
Molecular Weight:389.567
Hs Code.:

Synonyms:3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

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Chemical Property of 3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

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Technology Process of 3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

There total 1 articles about 3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 88818-05-7
3-benzyloxycarbonyl-2-oxa-3-azabicyclo<2.2.2>oct-5-ene-1-methanol

: 108634-78-2
3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87377-4

Reference yield: 94.0%

: 108634-78-2
3-benzyloxycarbonyl-1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

: 108634-81-7
(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butyldimethylsilyl)oxy>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

Guidance literature:: With potassium permanganate; tetra(n-butyl)ammonium hydrogensulfate; In water; benzene; Ambient temperature;
DOI:10.1016/S0040-4020(01)87377-4