2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

Base Information

Chemical Name:2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime
CAS No.:1349852-76-1
Molecular Formula:C₅₆H₈₆N₂O₁₆
Molecular Weight:1043.3
Hs Code.:

Synonyms:2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

Chemical Property:

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Technology Process of 2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

There total 2 articles about 2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1349852-75-0
2',4''-dibenzoyl-O-(2-methoxy-2-propyl)erythromycin A 9-oxime

: 74-88-4
methyl iodide

: C₅₇H₈₈N₂O₁₆

: 1349852-76-1
2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; for 0.666667h;

Reference yield:

: 114-07-8
erythromycin

: C₅₇H₈₈N₂O₁₆

: 1349852-76-1
2',4''-dibenzoyl-O-(2-methoxy-2-propyl)-6-O-methylerythromycin A 9-oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; triethylamine / methanol / Reflux

1.2: 1.25 h / 0 - 20 °C

2.1: dmap; triethylamine / ethyl acetate / 36 h / 20 °C

3.1: potassium hydroxide / tetrahydrofuran; dimethyl sulfoxide / 0.67 h / 0 - 20 °C

With dmap; hydroxylamine hydrochloride; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; dimethyl sulfoxide; ethyl acetate;