(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

Base Information

Chemical Name:(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol
CAS No.:1360864-29-4
Molecular Formula:C₃₅H₄₂N₂OSi
Molecular Weight:534.817
Hs Code.:

Synonyms:(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

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Technology Process of (R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

There total 4 articles about (R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1360864-28-3
tert-butyl ((1R,2R)-2-((5-(tert-butyl)-2-hydroxy-3-(triphenylsilyl)benzyl)amino)cyclohexyl)carbamate

: 1360864-29-4
(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201105079

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 1360864-29-4
(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol; water / 2 h / 20 °C / Inert atmosphere

2: methanol; 1,2-dichloro-ethane / Inert atmosphere

3: sodium tetrahydroborate / 6 h / 20 °C / Inert atmosphere

4: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; In methanol; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1002/anie.201105079

Reference yield:

: 146504-07-6
tert-butyl ((1R,2R)-2-aminocyclohexyl)carbamate

: 1360864-29-4
(R,R)-2-((2-aminocyclohexyl)amino)methyl-4-(tert-butyl)-6-(triphenylsilyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; 1,2-dichloro-ethane / Inert atmosphere

2: sodium tetrahydroborate / 6 h / 20 °C / Inert atmosphere

3: hydrogenchloride / ethyl acetate / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; In methanol; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1002/anie.201105079