C₂₅H₃₆N₄O₆S₂

Base Information

Chemical Name:C₂₅H₃₆N₄O₆S₂
CAS No.:936642-05-6
Molecular Formula:C₂₅H₃₆N₄O₆S₂
Molecular Weight:552.716
Hs Code.:

C<sub>25</sub>H<sub>36</sub>N<sub>4</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₂₅H₃₆N₄O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₆N₄O₆S₂

Chemical Property:

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Technology Process of C₂₅H₃₆N₄O₆S₂

There total 23 articles about C₂₅H₃₆N₄O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 936642-18-1
2-((4aS,5S,7S,8aR)-2,2,4a-trimethyl-7-((E)-4-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)but-1-en-1-yl)hexahydropyrano[4,3-d]-[1,3]dioxin-5-yl)ethanol

: 75-18-3
dimethylsulfide

: 936642-05-6
C₂₅H₃₆N₄O₆S₂

Guidance literature:: With dibenzoyl peroxide; In acetonitrile; at 0 - 20 ℃; for 1h;
DOI:10.1021/ol0701013

Reference yield:

: 936642-12-5
C₂₄H₂₉NO₄

: 936642-05-6
C₂₅H₃₆N₄O₆S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 85 percent / boric acid; H₂ / W-2 Raney nickel / H₂O; methanol / 6 h / 20 °C

2.1: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling

3.1: 98 percent / camphorsulfonic acid / 1 h / 20 °C

4.1: 96 percent / H₂ / Pd/C / methanol / 20 °C

5.1: 99 percent / imidazole / CH₂Cl₂ / 20 °C

6.1: 40 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C

7.1: Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

8.1: lithium hexamethyldisilazide / tetrahydrofuran / 0.5 h / 0 °C

8.2: 96 mg / tetrahydrofuran / 20 °C

9.1: 99 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

10.1: 81 percent / 2nd generation Grubbs' catalyst / CH₂Cl₂ / 22 h / 45 °C

11.1: 88 percent / benzoyl peroxide / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; boric acid; L-Selectride; Dess-Martin periodane; lithium hexamethyldisilazane; dibenzoyl peroxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium on activated charcoal; W-2 Raney nickel; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 7.1: Dess-Martin oxidation / 8.2: Wittig reaction;
DOI:10.1021/ol0701013

Reference yield:

: 936642-30-7
C₂₄H₂₉NO₅

: 936642-05-6
C₂₅H₃₆N₄O₆S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: zinc; aq. acetic acid / tetrahydrofuran / 0.08 h / 0 °C

2.1: 592 mg / sodium hypochlorite / H₂O; CH₂Cl₂ / 5 h / 20 °C

3.1: 85 percent / boric acid; H₂ / W-2 Raney nickel / H₂O; methanol / 6 h / 20 °C

4.1: 89 percent / L-selectride / tetrahydrofuran / 1 h / cooling

5.1: 98 percent / camphorsulfonic acid / 1 h / 20 °C

6.1: 96 percent / H₂ / Pd/C / methanol / 20 °C

7.1: 99 percent / imidazole / CH₂Cl₂ / 20 °C

8.1: 40 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C

9.1: Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

10.1: lithium hexamethyldisilazide / tetrahydrofuran / 0.5 h / 0 °C

10.2: 96 mg / tetrahydrofuran / 20 °C

11.1: 99 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

12.1: 81 percent / 2nd generation Grubbs' catalyst / CH₂Cl₂ / 22 h / 45 °C

13.1: 88 percent / benzoyl peroxide / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; sodium hypochlorite; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; boric acid; L-Selectride; Dess-Martin periodane; acetic acid; lithium hexamethyldisilazane; zinc; dibenzoyl peroxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium on activated charcoal; W-2 Raney nickel; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 9.1: Dess-Martin oxidation / 10.2: Wittig reaction;
DOI:10.1021/ol0701013