4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

Base Information

Chemical Name:4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide
CAS No.:1384840-69-0
Molecular Formula:C₂₉H₃₄N₂O₅S
Molecular Weight:522.665
Hs Code.:

Synonyms:4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

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Chemical Property of 4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

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Technology Process of 4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

There total 2 articles about 4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1384840-68-9
N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-4-(4-(1,3-dioxoisoindolin-2-yl)butoxy)-3-methoxy-N-phenylbenzenesulfonamide

: 1384840-69-0
4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

Guidance literature:: With hydrazine hydrate; In ethanol; dichloromethane; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/ml300042k

Reference yield:

: 927823-01-6
3,4-dimethoxy-N-[(2,2-dimethyl-2H-chromen-6-yl)methyl]-N-phenylbenzenesulfonamide

: 1384840-69-0
4-(4-aminobutoxy)-N-((2,2-dimethyl-2H-chromen-6-yl)methyl)-3-methoxy-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; thiophenol / 1-methyl-pyrrolidin-2-one / 0.5 h / 100 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

3: hydrazine hydrate / ethanol; dichloromethane / 3 h / Inert atmosphere; Reflux

With potassium carbonate; hydrazine hydrate; thiophenol; In 1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml300042k