(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

Base Information

Chemical Name:(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate
CAS No.:1622988-36-6
Molecular Formula:C₅₀H₆₆O₅
Molecular Weight:747.071
Hs Code.:

Synonyms:(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

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Chemical Property of (4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

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Technology Process of (4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

There total 3 articles about (4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1622988-34-4
(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-(triisopropylsilyloxy)-1,3-phenylene-didocosa-4,7,10,13,16,19-hexaenoate

: 1622988-36-6
(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1002/ejoc.201402282

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 1622988-36-6
(4,4',7,7',10,10',13,13',16,16',19,19'Z)-5-hydroxy-1,3-phenylenedidocosa-4,7,10,13,16,19-hexaenoate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / 20 °C

2: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 8 h / 20 °C

3: dicyclohexyl-carbodiimide; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

4: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 4 h / 20 °C

With dmap; triethylamine tris(hydrogen fluoride); dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201402282