triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride

Base Information

• Chemical Name: triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride
• CAS No.: 81175-96-4
• Molecular Formula: C₄₃H₃₇N₂O₂P₂*Cl
• Molecular Weight: 711.179

Synonyms:triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride

Chemical Property of triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride

Chemical Property:

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Technology Process of triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride

There total 4 articles about triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ⁵-dioxadiazaphosphorinan-6-yl)phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2,2,5-tetraphenyl-Δ4-1,3,4,2λ5-oxadiazaphospholine (55498-93-6) + triphenylphosphine (603-35-0) → triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ5-dioxadiazaphosphorinan-6-yl)phosphonium chloride (81175-96-4) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

With tetrachloromethane; In acetonitrile; for 3h; Ambient temperature;

Reference yield: 30.0%

5-phenyl-2H-1,2,3,4-tetrazole (18039-42-4) + triphenylphosphine (603-35-0) → triphenylchloromethylphosphonium perchlorate + triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ5-dioxadiazaphosphorinan-6-yl)phosphonium chloride (81175-96-4) + triphenylphosphazinephenyl-(5-phenyl-2-tetrazolyl)-methylene (81175-95-3)

Guidance literature:

With tetrachloromethane; triethylamine; In acetonitrile; at 30 - 40 ℃; for 4h;

Reference yield:

dichlorotriphenylphosphorane (2526-64-9) → triphenyl(2,2,2,4-tetraphenyl-1,3,5,6,2λ5-dioxadiazaphosphorinan-6-yl)phosphonium chloride (81175-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / acetonitrile; benzene; CCl₄ / 1 h / Ambient temperature

2: H₂O

With water; triethylamine; In tetrachloromethane; acetonitrile; benzene;

upstream raw materials:

5-phenyl-2H-1,2,3,4-tetrazole

triphenylphosphine

2,2,2,5-tetraphenyl-Δ⁴-1,3,4,2λ⁵-oxadiazaphospholine

N³-(p-Nitro-phenyl)-benzamidrazon

Downstream raw materials:

benzaldehyde

Triphenylphosphine oxide

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