methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

Base Information

Chemical Name:methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate
CAS No.:959861-51-9
Molecular Formula:C₁₄H₂₀O₂₀S₄
Molecular Weight:636.565
Hs Code.:

Synonyms:methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

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Technology Process of methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

There total 4 articles about methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 959861-59-7
methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

: 959861-51-9
methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

Guidance literature:: With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 40 ℃; for 16h;

Reference yield:

: 79250-48-9
methyl 2,5-bis(allyloxy)benzoate

: 959861-51-9
methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonamide; AD-mix-α / tert-butyl alcohol; water / 12 h / 0 °C

2: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 16 h / 40 °C

With methanesulfonamide; AD-mix-α; sulfur trioxide trimethylamine complex; In water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 2150-46-1
Methyl 2,5-dihydroxybenzoate

: 959861-51-9
methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 16 h / 25 °C

2.1: methanesulfonamide; AD-mix-α / tert-butyl alcohol; water / 12 h / 0 °C

3.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 16 h / 40 °C

With methanesulfonamide; AD-mix-α; sulfur trioxide trimethylamine complex; sodium hydride; In water; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;