methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

Base Information

• Chemical Name: methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate
• CAS No.: 959861-59-7
• Molecular Formula: C₁₄H₂₀O₈
• Molecular Weight: 316.308

Synonyms:methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

Chemical Property of methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

Chemical Property:

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Technology Process of methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate

There total 14 articles about methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl 2-(((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)-5-(((R)-2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)benzoate → methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate (959861-59-7)

Guidance literature:

With trifluoroacetic acid; In methanol; water; at 40 ℃; for 5h;

DOI:10.1002/ejoc.201901474

Reference yield: 97.0%

methyl 5-((S)-2,3-dihydroxypropoxy)-2-(((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)benzoate → methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate (959861-59-7)

Guidance literature:

With trifluoroacetic acid; In methanol; water; at 40 ℃; for 5h;

DOI:10.1002/ejoc.201901474

Reference yield: 61.0%

methyl 2,5-bis(allyloxy)benzoate (79250-48-9) → methyl 2-((R)-2,3-dihydroxypropoxy)-5-((S)-2,3-dihydroxypropoxy)benzoate (959861-59-7)

Guidance literature:

With AD-mix-α; methanesulfonamide; In water; tert-butyl alcohol; at 0 ℃; for 12h;

DOI:10.1016/j.bmcl.2007.08.074

upstream raw materials:

methyl 2,5-bis(allyloxy)benzoate

2,5-dihydroxybenzoic acid.

Methyl 2,5-dihydroxybenzoate

5-allyloxy-2-hydroxy-benzoic acid methyl ester

Downstream raw materials:

methyl 5-((R)-2,3-bis(sulfooxy)propoxy)-2-((S)-2,3-bis(sulfooxy)propoxy)benzoate

2,5-bis(allyloxy)benzoic acid

5-((R)-2,3-dihydroxypropoxy)-2-((S)-2,3-dihydroxypropoxy)benzoic acid

2-((R)-2,3-bis(sulfooxy)propoxy)-5-((S)-2,3-bis(sulfooxy)propoxy)benzoic acid

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