Technology Process of C29H38N8O10
There total 9 articles about C29H38N8O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; acetic acid;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 1h;
under 760 Torr;
DOI:10.1021/ja0293958
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diisopropylethylamine / CH2Cl2 / 1.5 h / 20 °C / Heating
2: diisopropylethylamine / CH2Cl2 / 0 - 20 °C
3: aq. HCl / ethyl acetate / pH 2
4: 2.2 g / DMAP; DCC / CH2Cl2 / 0 - 20 °C
5: 90 percent / TFA / CH2Cl2 / 1 h
6: H2; aq. AcOH / Pd/C / methanol / 1 h / 20 °C / 760 Torr
With
hydrogenchloride; dmap; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja0293958
- Guidance literature:
-
Multi-step reaction with 9 steps
1: DMAP / tetrahydrofuran / 1.5 h
2: 8.24 g / aq. KOH / tetrahydrofuran / 0.42 h / 20 °C
3: diisopropylethylamine / CH2Cl2 / 1.5 h / 20 °C / Heating
4: diisopropylethylamine / CH2Cl2 / 0 - 20 °C
5: aq. HCl / ethyl acetate / pH 2
6: 2.2 g / DMAP; DCC / CH2Cl2 / 0 - 20 °C
7: 90 percent / TFA / CH2Cl2 / 1 h
8: H2; aq. AcOH / Pd/C / methanol / 1 h / 20 °C / 760 Torr
With
hydrogenchloride; dmap; potassium hydroxide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja0293958
