1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

Base Information

Chemical Name:1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole
CAS No.:1337568-97-4
Molecular Formula:C₂₅H₃₅N
Molecular Weight:349.56
Hs Code.:

Synonyms:1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

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Chemical Property of 1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

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Technology Process of 1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

There total 4 articles about 1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1337568-79-2
6-methyl-8-(2,6,6-trimethylcyclohex-1-en-1-yl)octane-2,5-dione

: 100-46-9
benzylamine

: 1337568-97-4
1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

Guidance literature:: With acetic acid; In methanol; for 3h; Inert atmosphere; Molecular sieve; Reflux;
DOI:10.1021/ol202399c

Reference yield:

: 1337568-65-6
C₁₇H₃₀O₂

: 1337568-97-4
1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

2.2: 1 h / 20 °C / Inert atmosphere

3.1: acetic acid / methanol / 3 h / Inert atmosphere; Molecular sieve; Reflux

With dilauryl peroxide; sodium hydride; acetic acid; In methanol; dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1021/ol202399c

Reference yield:

: 1337568-67-8
2-[2-ethoxy-3-methyl-5-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-3-yl]-6-fluoropyridine

: 1337568-97-4
1-benzyl-2-methyl-5-(4-(2,6,6-trimethylcyclohex-1-en-1-yl)butan-2-yl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

1.2: 1 h / 20 °C / Inert atmosphere

2.1: acetic acid / methanol / 3 h / Inert atmosphere; Molecular sieve; Reflux

With dilauryl peroxide; acetic acid; In methanol; ethyl acetate;
DOI:10.1021/ol202399c