2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:702686-18-8
Molecular Formula:C₅₆H₅₉N₃O₁₂
Molecular Weight:966.097
Hs Code.:

Synonyms:2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of 2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of 2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 7 articles about 2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 702686-17-7
2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 702686-18-8
2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1023/B:RUBI.0000015775.24385.a0

Reference yield:

: 2-azidoethyl (4,6-O-benzylidene-β-D-galactopyranosyl)-(1→4)-β-D-glucopyranoside

: 702686-18-8
2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethylformamide / 4 h

2: 426 mg / trifluoroacetic acid / CHCl₃ / 0.5 h

3: 81 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; sodium hydride; trifluoroacetic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1023/B:RUBI.0000015775.24385.a0

Reference yield:

: 914772-35-3
(4aR,6S,7R,8S,8aS)-6-[(2R,3R,4S,5R,6R)-6-(2-Azido-ethoxy)-4,5-bis-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 702686-18-8
2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3-di-O-benzyl-6-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 426 mg / trifluoroacetic acid / CHCl₃ / 0.5 h

2: 81 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1023/B:RUBI.0000015775.24385.a0