diphenyl sec-pentyloxyphosphine

Base Information

• Chemical Name: diphenyl sec-pentyloxyphosphine
• CAS No.: 38011-61-9
• Molecular Formula: C₁₇H₂₁OP
• Molecular Weight: 272.327
• Mol file: 38011-61-9.mol

Synonyms:diphenyl sec-pentyloxyphosphine

Chemical Property of diphenyl sec-pentyloxyphosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenyl sec-pentyloxyphosphine

There total 1 articles about diphenyl sec-pentyloxyphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2-pentanol (6032-29-7,13403-73-1) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → diphenyl sec-pentyloxyphosphine (38011-61-9)

Guidance literature:

With 1-methyl-1H-imidazole; at 50 - 100 ℃; for 2h;

Reference yield: 94.9%

diphenyl sec-pentyloxyphosphine (38011-61-9) + mesitylene-2-carboxylic acid chloride (938-18-1) → (2,4,6-trimethylbenzoyl)diphenylphosphine oxide (75980-60-8)

Guidance literature:

at 50 - 90 ℃; for 7.33333h;

Reference yield:

diphenyl sec-pentyloxyphosphine (38011-61-9) → 2-iodopentane (637-97-8)

Guidance literature:

With hydrogen iodide;

DOI:10.1039/P19720001595

upstream raw materials:

(+/-)-2-pentanol

chloro-diphenylphosphine

Downstream raw materials:

2-methyl-1-chlorobutane

2-iodopentane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Refernces