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UV Photoinitiator TPO Omnirad TPO Irgacure TPO CAS No 75980-60-8
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TPO
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lower price TPO 75980-60-8 Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide
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Photoinitiator TPO
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diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS:75980-60-8
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Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide
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75980-60-8 Usage

Chemical Properties

white or cream powder

Uses

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide is a photo initiator, used in many kinds of ink industries
InChI:InChI=1/C22H21O2P/c1-16-14-17(2)21(18(3)15-16)22(23)25(24,19-10-6-4-7-11-19)20-12-8-5-9-13-20/h4-15H,1-3H3

75980-60-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

1.2 Other means of identification

Product number -
Other names diphenylphosphoryl-(2,4,6-trimethylphenyl)methanone

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Adhesives and sealant chemicals,Paint additives and coating additives not described by other categories,Processing aids, not otherwise listed
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:75980-60-8 SDS

75980-60-8Synthetic route

α-hydroxy-(2,4,6-trimethylbenzyl)diphenyl phosphine oxide

α-hydroxy-(2,4,6-trimethylbenzyl)diphenyl phosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With manganese(IV) oxide In dichloromethane at 20℃;98%
With vanadium(V) oxide; dihydrogen peroxide at 8 - 25℃; for 3.5h; Reagent/catalyst; Green chemistry;96%
With tert.-butylhydroperoxide In dichloromethane at 5 - 20℃; for 6.5h; Reagent/catalyst;92.5%
mesytaldehyde
487-68-3

mesytaldehyde

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: mesytaldehyde; Diphenylphosphine oxide In dichloromethane for 6h; Green chemistry;
Stage #2: With ammonium metavanadate; dihydrogen peroxide at 8 - 20℃; for 5.5h; Reagent/catalyst; Green chemistry;
98%
diphenyl n-pentyloxyphosphine
39150-04-4

diphenyl n-pentyloxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 9.33333h;95.8%
(sec-butyloxy)di(phenyl)phosphine
65119-90-6

(sec-butyloxy)di(phenyl)phosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;95.6%
Ethyl diphenylphosphinite
719-80-2

Ethyl diphenylphosphinite

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 40 - 90℃; for 8h; Time; Green chemistry;95.1%
With N,N-dimethyl-cyclohexanamine at 80 - 85℃; Product distribution / selectivity;
diphenyl n-propoxyphosphine
92556-46-2

diphenyl n-propoxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;95.1%
diphenyl sec-pentyloxyphosphine
38011-61-9

diphenyl sec-pentyloxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;94.9%
(n-butyloxy)di(phenyl)phosphine
13360-94-6

(n-butyloxy)di(phenyl)phosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 9.33333h;94.8%
(2,4,6-trimethylbenzyl)diphenylphosphine oxide
149731-53-3

(2,4,6-trimethylbenzyl)diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium In dichloromethane at 20℃;94%
ethanol
64-17-5

ethanol

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: ethanol With sodium In toluene at 65 - 70℃; for 2h;
Stage #2: chloro-diphenylphosphine In toluene at 5 - 10℃; for 1h;
Stage #3: mesitylene-2-carboxylic acid chloride In toluene at 70 - 75℃; for 5h; Temperature; Solvent;
92.2%
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: chloro-diphenylphosphine With potassium hydroxide In toluene at 20℃; for 2.5h; Inert atmosphere;
Stage #2: (trichloromethyl)mesitylene With iron(III) chloride at 90℃; Inert atmosphere;
91%
Stage #1: (trichloromethyl)mesitylene; chloro-diphenylphosphine With magnesium In tetrahydrofuran Reflux;
Stage #2: With hydrogenchloride; dihydrogen peroxide In water
87 g
isopropyl diphenylphosphinite
27350-46-5

isopropyl diphenylphosphinite

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;90.7%
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: (trichloromethyl)mesitylene; Diphenylphosphine oxide With iron(III) chloride In toluene at 90℃; for 3h; Inert atmosphere;
Stage #2: With water; sodium hydrogencarbonate In toluene at 20℃; Inert atmosphere;
89%
Stage #1: Diphenylphosphine oxide With n-butyllithium In tetrahydrofuran for 0.5h; Cooling with ice;
Stage #2: (trichloromethyl)mesitylene In tetrahydrofuran for 0.5h;
87%
Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

A

C34H32O3P2

C34H32O3P2

B

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With potassium hydroxide In 1,2-dichloro-ethane at -10℃; Solvent; Reagent/catalyst; Temperature; Inert atmosphere;A 8%
B 89%
Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dmap at 80℃;88.2%
With Methyltrichlorosilane; triethylamine In 1,4-dioxane at 60℃; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Green chemistry;71%
Stage #1: mesitylene-2-carboxylic acid chloride With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere;
Stage #2: Diphenylphosphine oxide In 1,2-dichloro-ethane for 5h; Reflux;
1.6 g
C22H21Cl2P

C22H21Cl2P

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dihydrogen peroxide In toluene84%
tetrachloromethane
56-23-5

tetrachloromethane

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere;
Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere;
Stage #3: Diphenylphosphine oxide In toluene Reagent/catalyst; Inert atmosphere;
84%
diphenylphosphinous acid methyl ester
4020-99-9

diphenylphosphinous acid methyl ester

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
81759-79-7

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 40 - 60℃;82%
Ethyl diphenylphosphinite
719-80-2

Ethyl diphenylphosphinite

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
81759-79-7

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 40 - 60℃;81%
tetrachloromethane
56-23-5

tetrachloromethane

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere;
Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere;
Stage #3: chloro-diphenylphosphine Further stages;
81%
mesytaldehyde
487-68-3

mesytaldehyde

benzene
71-43-2

benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: benzene With aluminum (III) chloride; phosphorus trichloride at 70 - 120℃;
Stage #2: mesytaldehyde at 5 - 10℃;
Stage #3: With tungsten trioxide; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide at 5 - 10℃; pH=2;
80%
1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride; hydrogenchloride / 2 h / 20 °C
2: magnesium / tetrahydrofuran / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride / 3 h / 20 - 45 °C
2.1: n-butyllithium / tetrahydrofuran / 0.5 h / Cooling with ice
2.2: 0.5 h
View Scheme
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 3 h / 20 - 45 °C
2.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere
2.2: 20 °C
3.1: dihydrogen peroxide / toluene
View Scheme
Multi-step reaction with 2 steps
1.1: C8H15N2(1+)*Br(1-)*2AlCl3; titanium tetrachloride; 1-methylimidazole hydrogen sulfate / 20 °C / 22502.3 - 30003 Torr / Autoclave
2.1: water; chlorobenzene / 2 h / 5 - 20 °C
2.2: 20 h / 5 °C / pH 3
View Scheme
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere
1.2: 20 °C
2.1: dihydrogen peroxide / toluene
View Scheme
2,4,6-trimethylbenzyl alcohol
4170-90-5

2,4,6-trimethylbenzyl alcohol

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dipotassium peroxodisulfate / acetone / 20 °C
2: manganese(IV) oxide / dichloromethane / 20 °C
View Scheme
mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

diphenyl(methyl)phosphine oxide
2129-89-7

diphenyl(methyl)phosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 0 - 80℃; for 3h; Inert atmosphere;
In toluene at 0 - 80℃; for 3h; Inert atmosphere;
benzene
71-43-2

benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride; trichlorophosphate / 4 h / 70 °C / Inert atmosphere
2: dmap / 80 °C
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride; trichlorophosphate / 70 - 120 °C
1.2: 0.5 h / 30 °C
2.1: toluene / 40 - 60 °C
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride; trichlorophosphate / 70 - 130 °C
1.2: 0.5 h / 30 °C
2.1: toluene / 40 - 60 °C
View Scheme
diphenylphosphanyl(2,4,6-trimethylphenyl)methanone

diphenylphosphanyl(2,4,6-trimethylphenyl)methanone

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dihydrogen peroxide In diethyl ether at 30 - 45℃; for 2h; Inert atmosphere;59.3g
With tert.-butylhydroperoxide; vanadia In chlorobenzene at 30℃; under 1500.15 Torr; for 0.00138889h; Temperature; Reagent/catalyst;
With 3-chloro-benzenecarboperoxoic acid In tetrahydrofuran at 25℃; for 3h; Inert atmosphere;
chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 35 - 60 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 45 - 65 °C
2: 9.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 50 - 100 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 50 - 65 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 3 h / 50 - 80 °C
2: 9.33 h / 50 - 90 °C
View Scheme
mesytaldehyde
487-68-3

mesytaldehyde

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorobenzene / 0 h / 30 °C / 1500.15 Torr
2: vanadia; tert.-butylhydroperoxide / chlorobenzene / 0 h / 30 °C / 1500.15 Torr
View Scheme
Stage #1: mesytaldehyde; chloro-diphenylphosphine In water; chlorobenzene at 5 - 20℃; for 2h;
Stage #2: With ammonium molibdate; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide In water; chlorobenzene at 5℃; for 20h; pH=3;
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

C25H24ClO3P

C25H24ClO3P

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h;99%
1-iodoperfluorododecane
307-60-8

1-iodoperfluorododecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

pentacosafluorododecyldiphenylphosphine
1424373-37-4

pentacosafluorododecyldiphenylphosphine

Conditions
ConditionsYield
With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation;98%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenyl(2,4,6-trimethylphenyl)phosphine oxide
91239-43-9

diphenyl(2,4,6-trimethylphenyl)phosphine oxide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 16h; Schlenk technique; Inert atmosphere;97%
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
With Diphenylphosphine oxide at 20℃; for 1.5h; Wavelength; Reagent/catalyst; Time; Inert atmosphere; Irradiation;96%
With diphenylphosphane at 20℃; for 3.5h; Wavelength; Irradiation; Inert atmosphere; Sealed tube;81 %Spectr.
In chloroform-d1 at 15 - 25℃; for 3.5h; Solvent; Irradiation; Sealed tube;41 %Spectr.
dodecafluoro-1,6-diiodohexane
375-80-4

dodecafluoro-1,6-diiodohexane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

1,6-bis(diphenylthiophosphinyl)perfluorohexane
1424373-26-1

1,6-bis(diphenylthiophosphinyl)perfluorohexane

Conditions
ConditionsYield
Stage #1: dodecafluoro-1,6-diiodohexane; (2,4,6-trimethylbenzoyl)diphenylphosphine oxide With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation;
Stage #2: With sulfur at 80℃; for 5h; Inert atmosphere;
96%
4,4'-dimethoxyphenyl disulfide
5335-87-5

4,4'-dimethoxyphenyl disulfide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

S-(4-methoxyphenyl) 2,4,6-trimethylthiobenzoate

S-(4-methoxyphenyl) 2,4,6-trimethylthiobenzoate

B

S-(4-methoxyphenyl)thiodiphenylphosphorus oxide
99234-85-2

S-(4-methoxyphenyl)thiodiphenylphosphorus oxide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 87%
B 96%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenyldisulfane
882-33-7

diphenyldisulfane

A

S-phenyl 2,4,6-trimethylthiobenzoate
50404-53-0

S-phenyl 2,4,6-trimethylthiobenzoate

B

diphenylthiophosphinic acid-S-phenyl ester
5510-78-1

diphenylthiophosphinic acid-S-phenyl ester

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 78%
B 95%
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenylphosphane
829-85-6

diphenylphosphane

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
at 20℃; for 1.5h; Irradiation;95%
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation; Sealed tube;88%
di(p-tolyl) disulfide
103-19-5

di(p-tolyl) disulfide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

S-(4-methylphenyl)thiodiphenylphosphorus oxide
5510-81-6

S-(4-methylphenyl)thiodiphenylphosphorus oxide

B

S-(4-methylphenyl) 2,4,6-trimethylthiobenzoate

S-(4-methylphenyl) 2,4,6-trimethylthiobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 94%
B 94%
bis(p-chlorophenyl) diselenide
20541-49-5

bis(p-chlorophenyl) diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

Se-(4-chlorophenyl) 2,4,6-trimethylselenobenzoate

Se-(4-chlorophenyl) 2,4,6-trimethylselenobenzoate

B

Se-(4-chlorophenyl) diphenylselenophosphinate

Se-(4-chlorophenyl) diphenylselenophosphinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 94%
B 92%
dibutyl diselenide
20333-40-8

dibutyl diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

P,P-diphenylphosphinoselenoic acid Se-butyl ester

P,P-diphenylphosphinoselenoic acid Se-butyl ester

B

Se-(n-butyl) 2,4,6-trimethylselenobenzoate

Se-(n-butyl) 2,4,6-trimethylselenobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 91%
B 94%
diphenyl diselenide
1666-13-3

diphenyl diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

Se-phenyl diphenylselenophosphinate
2049-62-9

Se-phenyl diphenylselenophosphinate

B

Se-phenyl 2,4,6-trimethylselenobenzoate

Se-phenyl 2,4,6-trimethylselenobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 92%
B 88%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

chloroacetyl chloride
79-04-9

chloroacetyl chloride

C24H22ClO3P

C24H22ClO3P

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h;92%
dibenzyl disulphide
150-60-7

dibenzyl disulphide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

diphenylphosphinothioic acid S-benzyl ester
3096-05-7

diphenylphosphinothioic acid S-benzyl ester

B

C17H18OS

C17H18OS

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 91%
B 40 %Spectr.
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
at 20℃; for 1.5h; Irradiation;90%
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation;90%
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