methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Base Information

Chemical Name:methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate
CAS No.:1373319-46-0
Molecular Formula:C₂₉H₃₅N₅O₇
Molecular Weight:565.626
Hs Code.:

Synonyms:methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Suppliers and Price of methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

There total 11 articles about methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1373319-42-6
methyl 3-isopropoxy-4-(6-isopropoxy-5-(6-isopropoxy-5-nitropicolinamido)picolinamido)benzoate

: 1373319-46-0
methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Guidance literature:: With tin(II) chloride dihdyrate; In ethyl acetate; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2ob07125h

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 1373319-46-0
methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 0.25 h / 0 °C

1.2: 16.25 h / 0 - 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 16 h / 120 °C / Inert atmosphere

3.1: potassium permanganate / water; acetone / 12 h / 20 °C

4.1: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

5.1: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

With potassium permanganate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tin(II) chloride dihdyrate; dichlorotriphenylphosphorane; In chloroform; water; ethyl acetate; acetone; toluene; 2.1: Stille coupling;
DOI:10.1039/c2ob07125h

Reference yield:

: 186413-80-9
2-isopropoxy-3-nitro-6-vinylpyridine

: 1373319-46-0
methyl 4-(5-(5-amino-6-isopropoxypicolinamido)-6-isopropoxypicolinamido)-3-isopropoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium permanganate / water; acetone / 12 h / 20 °C

2: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

3: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

With potassium permanganate; tin(II) chloride dihdyrate; dichlorotriphenylphosphorane; In chloroform; water; ethyl acetate; acetone;
DOI:10.1039/c2ob07125h