C₂₉H₃₄O₄S

Base Information

Chemical Name:C₂₉H₃₄O₄S
CAS No.:1315277-72-5
Molecular Formula:C₂₉H₃₄O₄S
Molecular Weight:478.653
Hs Code.:

C<sub>29</sub>H<sub>34</sub>O<sub>4</sub>S

Synonyms:C₂₉H₃₄O₄S

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Chemical Property of C₂₉H₃₄O₄S

Chemical Property:

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Technology Process of C₂₉H₃₄O₄S

There total 9 articles about C₂₉H₃₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1315278-19-3
(2R,3R)-6-benzyloxy-3-(4-methoxybenzyloxy)-2-methyl-1-hexanoic acid

: 106-45-6
para-thiocresol

: 1315277-72-5
C₂₉H₃₄O₄S

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.114

Reference yield:

: 935457-58-2
(2S,3R)-1-((4-methoxybenzyl)oxy)-2-methylhex-5-en-3-ol

: 1315277-72-5
C₂₉H₃₄O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / -10 °C / Inert atmosphere; Molecular sieve

2.1: tetrahydrofuran / 1.2 h / 20 °C / Inert atmosphere

3.1: dihydrogen peroxide; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 0 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

4.2: 0.67 h / 0 - 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.2 h / -78 - 0 °C / Inert atmosphere

5.2: 0.67 h / 0 - 20 °C

6.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.2 h / 0 - 20 °C

7.2: 0 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; potassium tert-butylate; dihydrogen peroxide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.03.114

Reference yield:

: 1315278-15-9
C₁₅H₂₂O₄

: 1315277-72-5
C₂₉H₃₄O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.67 h / 0 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.2 h / -78 - 0 °C / Inert atmosphere

2.2: 0.67 h / 0 - 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.2 h / 0 - 20 °C

4.2: 0 °C

5.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; potassium tert-butylate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dicyclohexyl-carbodiimide; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.03.114