5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

Base Information

Chemical Name:5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside
CAS No.:160243-11-8
Molecular Formula:C₃₃H₃₉NO₈
Molecular Weight:577.675
Hs Code.:

Synonyms:5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

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Chemical Property of 5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

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Technology Process of 5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

There total 1 articles about 5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-3-O-chloroacetyl-L-fucopyranoside

: 160243-11-8
5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

Guidance literature:: With thiourea; In methanol; at 40 ℃; for 72h;
DOI:10.1016/0008-6215(94)84179-9

Reference yield: 71.0%

: 68499-56-9
1,3,4,6-tetra-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranoside

: 160243-11-8
5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

: 160243-15-2
5-(benzyloxycarbonylamino)pentyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1<*>3)-4-O-benzoyl-α-L-fucopyranoside

Guidance literature:: With iron(III) chloride; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/0008-6215(94)84179-9

Reference yield:

: 160243-11-8
5-(benzyloxycarbonylamino)pentyl 4-O-benzoyl-2-O-benzyl-α-L-fucopyranoside

: Benzoic acid (2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-6-(5-amino-pentyloxy)-5-hydroxy-2-methyl-tetrahydro-pyran-3-yl ester; compound with acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / FeCl₃ / CH₂Cl₂ / 24 h / Ambient temperature

2: 93 percent / Zn, AcOH / 3 h / Ambient temperature

3: 100 percent / NaOMe / methanol / 96 h / Ambient temperature

4: 100 percent / H₂ / 10percent Pd/C / methanol; H₂O / 24 h / Ambient temperature

With hydrogen; sodium methylate; iron(III) chloride; acetic acid; zinc; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1016/0008-6215(94)84179-9