1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

Base Information

• Chemical Name: 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine
• CAS No.: 115031-66-8
• Molecular Formula: C₂₄H₃₇N
• Molecular Weight: 339.564

Synonyms:1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

Chemical Property of 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

Chemical Property:

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Technology Process of 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

There total 4 articles about 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

13-cis-vitamin A aldehyde (472-86-6) + N-butylamine (109-73-9,85404-21-3) → butyl-(13Z,15E)-retinylidene-amine (68737-92-8) + trans-N-retinylidene-n-butylimine (36076-04-7,51804-54-7,51847-39-3,52647-48-0,61769-47-9,68737-92-8,68737-93-9,68737-94-0,74644-89-6,80736-10-3,92216-30-3,98462-61-4,100836-89-3,120201-10-7,34512-76-0) + 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115031-66-8)

Guidance literature:

With 4 A molecular sieve; In ethanol; 1) 0 deg C, 1 h; 2) rt, 1 h;

DOI:10.1021/ja00221a084

Reference yield:

13-cis-vitamin A aldehyde (472-86-6) + N-butylamine (109-73-9,85404-21-3) → butyl-(13Z,15Z)-retinylidene-amine (92216-30-3) + 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115031-66-8)

Guidance literature:

With 4 A molecular sieve; In ethanol; at 0 ℃; Title compound not separated from byproducts;

DOI:10.1021/ja00193a043

Reference yield:

trans-N-retinylidene-n-butylimine (36076-04-7,51804-54-7,51847-39-3,52647-48-0,61769-47-9,68737-92-8,68737-93-9,68737-94-0,74644-89-6,80736-10-3,92216-30-3,98462-61-4,100836-89-3,120201-10-7,34512-76-0) → butyl-(9Z,15E)-retinylidene-amine (68737-94-0) + butyl-(13Z,15Z)-retinylidene-amine (92216-30-3) + 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115031-66-8)

Guidance literature:

In benzene-d6; at 78 ℃; for 0.5h; Product distribution; other time;

DOI:10.1021/ja00193a043

upstream raw materials:

trans-N-retinylidene-n-butylimine

butyl-(13Z,15Z)-retinylidene-amine

13-cis-vitamin A aldehyde

N-butylamine

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