α--α-isonitrosoacetone

Base Information

• Chemical Name: α--α-isonitrosoacetone
• CAS No.: 85914-46-1
• Molecular Formula: C₁₁H₁₅N₃O₂
• Molecular Weight: 221.259

Synonyms:α--α-isonitrosoacetone

Chemical Property of α--α-isonitrosoacetone

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of α--α-isonitrosoacetone

There total 1 articles about α--α-isonitrosoacetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

pyruvohydroximoyl chloride (5471-68-1) + 4-amino-N,N-dimethylaniline (99-98-9) → α--α-isonitrosoacetone (85914-46-1)

Guidance literature:

With triethylamine; In diethyl ether; for 3h;

DOI:10.1007/BF00765163

Reference yield: 81.5%

α--α-isonitrosoacetone (85914-46-1) → N-(4-Dimethylamino-phenyl)-2-hydrazono-N'-hydroxy-propionamidine (85914-40-5)

Guidance literature:

With hydrazine hydrate; In ethanol; 1.) reflux, 7 min, 2.) 3 h, room temp.;

DOI:10.1007/BF00765163

Reference yield: 61.0%

thiosemicarbazide hydrochloride (4346-94-5) + α--α-isonitrosoacetone (85914-46-1) → C12H18N6OS (100098-14-4)

Guidance literature:

With sodium hydroxide; In ethanol; for 0.166667h; Ambient temperature;

DOI:10.1007/BF00763717

upstream raw materials:

pyruvohydroximoyl chloride

4-amino-N,N-dimethylaniline

Downstream raw materials:

C₁₂H₁₈N₆OS

N-(4-Dimethylamino-phenyl)-2-hydrazono-N'-hydroxy-propionamidine

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