N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester
CAS No.:167170-11-8
Molecular Formula:C₁₄H₁₈BrNO₄
Molecular Weight:344.205
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

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Chemical Property of N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

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Technology Process of N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

There total 9 articles about N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 141406-83-9
methyl (2S)-2-[N-(benzyloxycarbonyl)amino]-5-(hydroxy)pentanoate

: 167170-11-8
N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/ol3030583

Reference yield: 67.0%

: 5672-83-3
Z-L-GluOMe

: 167170-11-8
N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

Guidance literature:: Z-L-GluOMe; With chloroformic acid ethyl ester;

With sodium tetrahydroborate; In methanol;

With carbon tetrabromide; triphenylphosphine;
DOI:10.1016/S0040-4039(03)01222-X

Reference yield:

: 13907-82-9,2650-67-1
N²-benzyloxycarbonyl-L-glutamine methyl ester

: 167170-11-8
N-(benzyloxycarbonyl)-5-bromonorvaline methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: tBuONO

2.1: ClCOOEt

2.2: NaBH₄ / methanol

2.3: 67 percent / CBr₄; PPh₃

With tert.-butylnitrite; chloroformic acid ethyl ester;
DOI:10.1016/S0040-4039(03)01222-X