3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid

Base Information

• Chemical Name: 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid
• CAS No.: 1013659-10-3
• Molecular Formula: C₉H₆Br₂O₃S
• Molecular Weight: 354.019
• Mol file: 1013659-10-3.mol

Synonyms:3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid

Chemical Property of 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid

There total 3 articles about 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-(3,5-dibromo-2-hydroxybenzylidene)-2-thioxothiazolidin-4-one → 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid (1013659-10-3)

Guidance literature:

5-(3,5-dibromo-2-hydroxybenzylidene)-2-thioxothiazolidin-4-one; With sodium hydroxide;

With hydrogenchloride;

DOI:10.1039/b501309g

Reference yield: 95.0%

2-thioxo-4-thiazolidinone (141-84-4) + 3,5-Dibromosalicylaldehyde (90-59-5) → 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid (1013659-10-3)

Guidance literature:

Multistep reaction;

DOI:10.1002/ejic.200500237

Reference yield:

3,5-Dibromosalicylaldehyde (90-59-5) → 3-(3,5,-dibromo-2hydroxyphenyl)-2-sulfanylpropenoic acid (1013659-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aq. NaOH

1.2: 95 percent / aq. HCl

With sodium hydroxide;

DOI:10.1039/b501309g

upstream raw materials:

2-thioxo-4-thiazolidinone

3,5-Dibromosalicylaldehyde

Downstream raw materials:

(3-thio-2H-6,8-dibromo-1-benzopyran-2-one)triphenyltin(IV)

C₁₅H₂₀AuBr₂O₃PS

C₂₁H₃₄Au₂Br₂O₃P₂S

bis(triethylphosphine)digold(I) 3-(3,5-dibromo-2-hydroxyphenyl)-2-sulfanylpropenoate