3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Base Information

Chemical Name:3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate
CAS No.:611217-61-9
Molecular Formula:C₃₁H₄₁ClO₈
Molecular Weight:577.115
Hs Code.:

3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Synonyms:3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Suppliers and Price of 3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

There total 2 articles about 3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 7381-30-8
2,2,7,7-tetramethyl-3,6-dioxa-2,7-disilaoctane

: 462125-47-9
3-acetoxy-4-chloro-6-formyl-5-methyl-2-[(2E,4E)-3-methyl-5-((1R,2R,6R)-1,2,6-trimethyl-3-oxocyclohexyl)-2,4-pentadienyl]phenyl acetate

: 611217-61-9
3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 0 ℃; for 2h;
DOI:10.1021/jm0205649

Reference yield:

: 26166-39-2
Ascochlorin

: 611217-61-9
3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / 4 h / 20 °C

2: 33 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 2 h / -78 - 0 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jm0205649

Reference yield:

: 611217-61-9
3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(2E,4E)-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

: 611217-63-1
3-acetoxy-4-chloro-6-(1,3-dioxolan-2-yl)-5-methyl-2-[(E)-2,3-epoxy-3-methyl-5-((6R,7R,8R)-6,7,8-trimethyl-1,4-dioxaspiro[4.5]dec-7-yl)-2,4-pentadienyl]phenyl acetate

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1.5h; cooling;
DOI:10.1021/jm0205649