2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

Base Information

Chemical Name:2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene
CAS No.:1434816-99-5
Molecular Formula:C₂₈H₂₂ClF₃OS
Molecular Weight:498.996
Hs Code.:

Synonyms:2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

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Chemical Property of 2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

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Technology Process of 2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

There total 2 articles about 2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 374-01-6,17556-48-8,17628-73-8,3539-97-7
(S)-1,1,1-trifluoro-2-propanol

: 1434816-93-9
2-chloro-4-fluoro-1-tritylsulfanylbenzene

: 1434816-99-5
2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

Guidance literature:: (S)-1,1,1-trifluoro-2-propanol; With sodium t-butanolate; In N,N-dimethyl acetamide; at 2 ℃; for 0.25h;

2-chloro-4-fluoro-1-tritylsulfanylbenzene; In N,N-dimethyl acetamide; at 50 ℃; for 3h;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 175277-99-3
2-chloro-4-fluorobenzenethiol

: 1434816-99-5
2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice

2.1: sodium t-butanolate / N,N-dimethyl acetamide / 0.25 h / 2 °C

2.2: 3 h / 50 °C

With trifluoroacetic acid; sodium t-butanolate; In dichloromethane; N,N-dimethyl acetamide;

Reference yield: 93.0%

: 1434816-99-5
2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene

: 1434816-87-1
2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)benzenethiol

Guidance literature:: 2-chloro-4-((S)-2,2,2-trifluoro-1-methylethoxy)-1-tritylsulfanyl benzene; With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Cooling with ice;

With potassium hydroxide; In dichloromethane; water; for 0.25h;