C₂₇H₃₂N₆O₂

Base Information

Chemical Name:C₂₇H₃₂N₆O₂
CAS No.:1253409-08-3
Molecular Formula:C₂₇H₃₂N₆O₂
Molecular Weight:472.59
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:C₂₇H₃₂N₆O₂

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Chemical Property of C₂₇H₃₂N₆O₂

Chemical Property:

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Technology Process of C₂₇H₃₂N₆O₂

There total 7 articles about C₂₇H₃₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.4%

: 1209490-20-9
C₁₅H₁₇N₅O

: 104177-71-1
o-isopentylaniline

: 7693-46-1
4-Nitrophenyl chloroformate

: 1253409-08-3
C₂₇H₃₂N₆O₂

Guidance literature:: C₁₅H₁₇N₅O; 4-Nitrophenyl chloroformate; With pyridine; In dichloromethane; at 20 ℃; for 2.5h; Inert atmosphere; Cooling with ice;

o-isopentylaniline; With triethylamine; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 1209528-84-6
C₁₃H₁₄N₄O₂

: 1253409-08-3
C₂₇H₃₂N₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos / 1,2-dimethoxyethane / 3 h / Inert atmosphere; Reflux

2.1: formic acid / palladium on activated carbon / methanol / 2 h / Inert atmosphere; Reflux

2.2: 20 °C

2.3: 0.5 h / 20 °C

3.1: pyridine / dichloromethane / 2.5 h / 20 °C / Inert atmosphere; Cooling with ice

3.2: 24 h / 20 °C

With pyridine; potassium phosphate; formic acid; palladium on activated carbon; bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos; In methanol; 1,2-dimethoxyethane; dichloromethane;

Reference yield:

: 1200497-67-1
C₁₂H₁₇N₃O₄

: 1253409-08-3
C₂₇H₃₂N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1.5 h / 20 °C

2.1: triethylamine; diphenyl phosphoryl azide / toluene / 5.5 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 4 h / 40 - 60 °C

3.2: 16.5 h / 20 °C

4.1: potassium phosphate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos / 1,2-dimethoxyethane / 3 h / Inert atmosphere; Reflux

5.1: formic acid / palladium on activated carbon / methanol / 2 h / Inert atmosphere; Reflux

5.2: 20 °C

5.3: 0.5 h / 20 °C

6.1: pyridine / dichloromethane / 2.5 h / 20 °C / Inert atmosphere; Cooling with ice

6.2: 24 h / 20 °C

With pyridine; hydrogenchloride; potassium phosphate; formic acid; diphenyl phosphoryl azide; water; triethylamine; lithium hydroxide; palladium on activated carbon; bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; toluene;