4-Bromo-n-propylbenzenesulfonamide

Base Information

Chemical Name:4-Bromo-n-propylbenzenesulfonamide
CAS No.:3476-19-5
Molecular Formula:C9H12BrNO2S
Molecular Weight:278.17
Hs Code.:2935009090
NSC Number:406257
DSSTox Substance ID:DTXSID80188310
Nikkaji Number:J54.919C
Wikidata:Q83060125
Mol file:3476-19-5.mol

Synonyms:4-bromo-n-propylbenzenesulfonamide;3476-19-5;p-Bromo-N-propylbenzenesulfonamide;Benzenesulfonamide, p-bromo-N-propyl-;Benzenesulfonamide, 4-bromo-N-propyl-;NSC 406257;BRN 3135139;4-bromo-N-propylbenzene-1-sulfonamide;NSC406257;WLN: ER DSWM3;Oprea1_720730;SCHEMBL3019231;DTXSID80188310;4-bromo-N-propyl-benzenesulfonamide;4-BroMo-N-n-propylbenzenesulfonaMide;MFCD01215072;AKOS003835712;NSC-406257;BS-25155;LS-31325;CS-0209155;F15490;EN300-1452837;A874868;AP-263/11658295;Z45545162

Suppliers and Price of 4-Bromo-n-propylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-N-propylbenzenesulfonamide
250mg
$ 55.00

Crysdot
4-Bromo-N-propylbenzenesulfonamide 95+%
10g
$ 355.00

Crysdot
4-Bromo-N-propylbenzenesulfonamide 95+%
25g
$ 640.00

Alichem
4-Bromo-N-propylbenzenesulfonamide
10g
$ 375.90

AK Scientific
4-Bromo-N-propylbenzenesulfonamide
25g
$ 957.00

Total 13 raw suppliers

Chemical Property of 4-Bromo-n-propylbenzenesulfonamide

Chemical Property:

Vapor Pressure:3.17E-05mmHg at 25°C
Boiling Point:355.2°C at 760 mmHg
Flash Point:168.6°C
PSA：54.55000
Density:1.47g/cm³
LogP:3.60910
Storage Temp.:2-8°C
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:276.97721
Heavy Atom Count:14
Complexity:253

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-N-propylbenzenesulfonamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCNS(=O)(=O)C1=CC=C(C=C1)Br

Technology Process of 4-Bromo-n-propylbenzenesulfonamide

There total 5 articles about 4-Bromo-n-propylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1-((4-bromophenyl)sulfonyl)-1H-benzo[d][1,2,3]triazole

: 108-03-2
1-Nitropropane

: 3476-19-5
4-bromo-N-propylbenzenesulfonamide

Guidance literature:: With chloro-trimethyl-silane; (1,2-dimethoxyethane)dichloronickel(II); bathophenanthroline; zinc; In 1,4-dioxane; at 100 ℃; for 15h; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.1c03535

Reference yield: 28.0%

: 107-10-8,42939-71-9
propylamine

: 98-58-8
4-bromobenzenesulfonyl chloride

: 3476-19-5
4-bromo-N-propylbenzenesulfonamide

Guidance literature:: In dichloromethane; for 16h; Sealed tube;

Reference yield:

: 98-58-8
4-bromobenzenesulfonyl chloride

: 3476-19-5
4-bromo-N-propylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 10 h / Inert atmosphere

2: (1,2-dimethoxyethane)dichloronickel(II); bathophenanthroline; zinc; chloro-trimethyl-silane / 1,4-dioxane / 15 h / 100 °C / Schlenk technique; Sealed tube; Inert atmosphere

With chloro-trimethyl-silane; (1,2-dimethoxyethane)dichloronickel(II); bathophenanthroline; triethylamine; zinc; In 1,4-dioxane; dichloromethane;
DOI:10.1021/acs.orglett.1c03535