N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide

Base Information

• Chemical Name: N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide
• CAS No.: 66666-34-0
• Molecular Formula: C₂₀H₂₂N₄O₅S
• Molecular Weight: 430.484

Synonyms:N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide

Chemical Property of N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide

Chemical Property:

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Technology Process of N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide

There total 2 articles about N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one (7692-38-8) → 2-Methoxybenzoic acid (579-75-9) + 2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-hydroxy-2'-methylene-4'-(2-methoxyphenyl)-tetrahydropyrrol-5'-one> (74982-37-9) + N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide (66666-34-0)

Guidance literature:

With dihydrogen peroxide; In acetic acid; for 56h; Ambient temperature;

DOI:10.1248/cpb.28.769

Reference yield:

→ N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide (66666-34-0)

Guidance literature:

2-o-Methoxyphenyl-4-<(2-methyl-4-aminopyrimidin-5-yl)-methyl>-5-methyl-6-(2-hyd-roxyethyl)-3-oxo-2.3-dihydro-4H-1.4-thiazin (Id), m-Chlorperbenzoesaeure;

DOI:10.1248/cpb.26.722

Reference yield: 36.0%

N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide (66666-34-0) → 2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-hydroxy-2'-methylene-4'-(2-methoxyphenyl)-tetrahydropyrrol-5'-one> (74982-37-9)

Guidance literature:

In acetic acid; for 48h;

DOI:10.1248/cpb.28.769

upstream raw materials:

4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one

Downstream raw materials:

2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-hydroxy-2'-methylene-4'-(2-methoxyphenyl)-tetrahydropyrrol-5'-one>

2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-methoxy-2'-methylene-4'-(2-methoxyphenyl)tetrahydropyrrol-5'-one>

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