3-chlorophenethyl azide

Base Information

• Chemical Name: 3-chlorophenethyl azide
• CAS No.: 1316652-69-3
• Molecular Formula: C₈H₈ClN₃
• Molecular Weight: 181.625
• Mol file: 1316652-69-3.mol

Synonyms:3-chlorophenethyl azide

Chemical Property of 3-chlorophenethyl azide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-chlorophenethyl azide

There total 5 articles about 3-chlorophenethyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(3-chlorophenyl)ethyl bromide (16799-05-6) → 3-chlorophenethyl azide (1316652-69-3)

Guidance literature:

With sodium azide; In dimethyl sulfoxide;

DOI:10.1021/jm300837y

Reference yield: 80.0%

→ 3-chlorophenethyl azide (1316652-69-3)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 20 ℃; for 5h;

Reference yield: 57.0%

2-(3-chlorophenyl)ethylamine (13078-79-0) → 3-chlorophenethyl azide (1316652-69-3)

Guidance literature:

With triflic azide; copper(II) sulfate; triethylamine; In methanol; dichloromethane; water; at 20 ℃; Cooling with ice;

DOI:10.1002/anie.201609655

upstream raw materials:

2-(3-chlorophenyl)ethyl bromide

2-(3-chlorophenyl)ethylamine

2-(3-chlorophenyl)ethanol

Downstream raw materials:

C₁₇H₁₅ClN₄O₂

C₂₃H₂₀ClN₅O

m-Chlorophenylethylamine hydrochloride