(E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate

Base Information

Chemical Name:(E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate
CAS No.:107445-22-7
Molecular Formula:C₁₄H₁₄N₂O₃S
Molecular Weight:290.343
Hs Code.:
DSSTox Substance ID:DTXSID901179683

Synonyms:107445-22-7;[(E)-1-Pyridin-4-ylethylideneamino] 4-methylbenzenesulfonate;(E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate;SCHEMBL7296406;DTXSID901179683;EN300-1587544;(1E)-1-(4-Pyridinyl)ethanone O-[(4-methylphenyl)sulfonyl]oxime

Suppliers and Price of (E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:290.07251349
Heavy Atom Count:20
Complexity:428

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)ON=C(C)C2=CC=NC=C2
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)O/N=C(\C)/C2=CC=NC=C2

Technology Process of (E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate

There total 2 articles about (E)-[1-(pyridin-4-yl)ethylidene]amino 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107445-21-6
(E)-1-(pyridin-4-yl)ethan-1-one oxime

: 98-59-9
p-toluenesulfonyl chloride

: 107445-22-7
(E)-1-(pyridin-4-yl)ethanone O-tosyloxime

Guidance literature:: With pyridine; at 25 ℃; for 24h;
DOI:10.15227/orgsyn.064.0019

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1194-99-6
4-acetylpyridine oxime

: 107445-22-7
(E)-1-(pyridin-4-yl)ethanone O-tosyloxime

Guidance literature:: With pyridine;
DOI:10.1039/jr9550004315

Reference yield: 74.5%

: 64-17-5
ethanol

: 107445-22-7
(E)-1-(pyridin-4-yl)ethanone O-tosyloxime

: 74209-44-2
2,2-diethoxy-2-(4-pyridiyl)ethylamine

Guidance literature:: ethanol; (E)-1-(pyridin-4-yl)ethanone O-tosyloxime; With potassium; In ethanol; at 0 - 20 ℃; for 1.25h;

With hydrogenchloride; In diethyl ether; for 0.25h;

With sodium carbonate; In water; pH=> 10;
DOI:10.15227/orgsyn.064.0019