(2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide

Base Information

• Chemical Name: (2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide
• CAS No.: 1011506-17-4
• Molecular Formula: C₃₇H₅₀O₂S₂
• Molecular Weight: 590.935

Synonyms:(2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide

Chemical Property of (2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide

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Technology Process of (2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide

There total 1 articles about (2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C31H46O2S (190958-71-5) + 4-bromo-3-methyl-2-butenyl phenyl sulfide (359010-59-6) → (2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide (1011506-17-4)

Guidance literature:

C₃₁H₄₆O₂S; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

4-bromo-3-methyl-2-butenyl phenyl sulfide; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Further stages.;

DOI:10.1021/jo702303a

Reference yield: 75.0%

(2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide (1011506-17-4) → (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene (1011506-23-2)

Guidance literature:

With LiNbMoO₆; dihydrogen peroxide; In methanol; benzene; for 11h; cooling;

DOI:10.1021/jo702303a

upstream raw materials:

C₃₁H₄₆O₂S

4-bromo-3-methyl-2-butenyl phenyl sulfide

Downstream raw materials:

(2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene

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