(2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene

Base Information

• Chemical Name: (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene
• CAS No.: 1011506-23-2
• Molecular Formula: C₃₇H₅₀O₄S₂
• Molecular Weight: 622.934

Synonyms:(2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene

Chemical Property of (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene

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Technology Process of (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene

There total 1 articles about (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide (1011506-17-4) → (2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene (1011506-23-2)

Guidance literature:

With LiNbMoO₆; dihydrogen peroxide; In methanol; benzene; for 11h; cooling;

DOI:10.1021/jo702303a

Reference yield:

(2E,6E,10E,14E)-1,5-bis(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaene (1011506-23-2) → (2E,6E)-1,5-bis(benzenesulfonyl)-3,7-dimethyl-9-(2,5,5,8a-tetramethyl-1,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl)nona-2,6-diene + (2E,6E)-1,5-bis(benzenesulfonyl)-3,7-dimethyl-9-(2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl)nona-2,6-diene (1011717-98-8)

Guidance literature:

With methanesulfonic acid; In various solvent(s); at 20 ℃; for 0.5h;

DOI:10.1021/jo702303a

upstream raw materials:

(2E,6E,10E,14E)-5-(benzenesulfonyl)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl phenyl sulfide

Downstream raw materials:

(2E,6E)-1,5-bis(benzenesulfonyl)-3,7-dimethyl-9-(2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl)nona-2,6-diene

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