pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

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Chemical Name:pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene
CAS No.:383404-41-9
Molecular Formula:C₃₃H₃₇N₃Si
Molecular Weight:503.762
Hs Code.:

Synonyms:pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

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Chemical Property of pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

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Technology Process of pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

There total 1 articles about pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 214628-10-1
2-(triisopropylsilylethynyl)-1-(6-trimethylsilyl-1,3,5-hexatriynyl)benzene

: 250160-25-9
N,N-tetramethylene-N'-(2'-iodophenyl)triazene

: 383404-41-9
pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

Guidance literature:: With potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; triethylamine; at 60 ℃;
DOI:10.1002/1099-0690(200109)2001:18<3485::AID-EJOC3485>3.0.CO;2-I

Reference yield: 82.0%

: 383404-41-9
pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

: 74-88-4
methyl iodide

: 214628-09-8
{2-[6-(2-Iodo-phenyl)-hexa-1,3,5-triynyl]-phenylethynyl}-triisopropyl-silane

Guidance literature:: at 120 ℃; for 12h;
DOI:10.1002/1099-0690(200109)2001:18<3485::AID-EJOC3485>3.0.CO;2-I

Reference yield:

: 383404-41-9
pyrrolidin-1-yl-[2-(6-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hexa-1,3,5-triynyl)-phenyl]-diazene

: 214628-18-9
C₅₂H₅₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 12 h / 120 °C

2: 20 percent / aq. KOH / PdCl₂(PPh₃)2; CuI / tetrahydrofuran; triethylamine / 60 °C

With potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; triethylamine;
DOI:10.1002/1099-0690(200109)2001:18<3485::AID-EJOC3485>3.0.CO;2-I