benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

Base Information

Chemical Name:benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate
CAS No.:106880-75-5
Molecular Formula:C₃₂H₃₈N₂O₈
Molecular Weight:578.662
Hs Code.:

benzyl <<<o-<(2-methoxyethoxy)methoxy>benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

Synonyms:benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

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Chemical Property of benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

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Technology Process of benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

There total 7 articles about benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19165-29-8
N-(trifluoroacetyl)anthranilic acid

: 106880-75-5
benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N,N'-carbonylbisimidazole / 1.) 2 h, RT; 2.) tert-butyl alcohol, 36 h, RT, and ethanol, sodium borohydride, 0 deg C, ca. 25 min

2: 82 percent / acetic acid, sodium cyanoborohydride / methanol / Ambient temperature

3: 1.) NaH / 1.) toluene, RT;

With sodium hydride; sodium cyanoborohydride; acetic acid; 1,1'-carbonyldiimidazole; In methanol;
DOI:10.1021/ja00240a036

Reference yield:

: 64113-91-3
tert-butyl 2-aminobenzoate

: 106880-75-5
benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / acetic acid, sodium cyanoborohydride / methanol / Ambient temperature

2: 1.) NaH / 1.) toluene, RT;

With sodium hydride; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1021/ja00240a036

Reference yield:

: 106880-69-7
o-<(2-methoxyethoxy)methoxy>benzaldehyde

: 106880-75-5
benzyl <<benzyl>((tert-butoxycarbonyl)phenyl)carbamoyl>methyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / acetic acid, sodium cyanoborohydride / methanol / Ambient temperature

2: 1.) NaH / 1.) toluene, RT;

With sodium hydride; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1021/ja00240a036