2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

Base Information

Chemical Name:2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside
CAS No.:77667-33-5
Molecular Formula:C₂₅H₃₂N₃O₁₁
Molecular Weight:550.543
Hs Code.:

Synonyms:2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

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Chemical Property of 2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

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Technology Process of 2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

There total 4 articles about 2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 77667-30-2
4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)-2-nitrophenyl2,3,4-tri-O-acetyl-β-D-fucopyranoside

: 77667-33-5
2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

Guidance literature:: With lead dioxide; In benzene; Ambient temperature;
DOI:10.1016/S0008-6215(00)85536-6

Reference yield:

: 5158-64-5,14227-85-1,16741-27-8,24877-07-4,36807-84-8,39524-38-4,41881-45-2,60978-06-5,69483-13-2,69980-52-5,75247-28-8,75247-29-9,80483-13-2,80483-14-3,89301-86-0,96648-29-2,108942-35-4,108942-38-7,138514-69-9,24404-52-2
2,3,4-tri-O-acetyl-D-fucopyranosyl bromide

: 77667-33-5
2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / 1M sodium hydroxide / acetone / Ambient temperature

2: 56 percent / benzene / 24 h / Ambient temperature

3: 71 percent / lead(IV)dioxide / benzene / Ambient temperature

With sodium hydroxide; lead dioxide; In acetone; benzene;
DOI:10.1016/S0008-6215(00)85536-6

Reference yield:

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 77667-33-5
2-nitro-4-(4,4,5,5-tetramethylimidazolidin-2-yl 1-oxide)phenyl-2,3,4-tri-O-acetyl-β-D-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / 1M sodium hydroxide / acetone / Ambient temperature

2: 56 percent / benzene / 24 h / Ambient temperature

3: 71 percent / lead(IV)dioxide / benzene / Ambient temperature

With sodium hydroxide; lead dioxide; In acetone; benzene;
DOI:10.1016/S0008-6215(00)85536-6