methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

Base Information

Chemical Name:methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate
CAS No.:169616-96-0
Molecular Formula:C₂₄H₃₇NS₂
Molecular Weight:403.696
Hs Code.:

Synonyms:methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

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Technology Process of methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

There total 4 articles about methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75-15-0,12122-00-8
carbon disulfide

: 169616-93-7
N-methyl-4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]aniline

: 74-88-4
methyl iodide

: 169616-96-0
methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

Guidance literature:: With n-butyllithium;
DOI:10.1246/cl.1995.683

Reference yield:

: 1-phenyl-trans-4-(trans-4-propylcyclohexyl)cyclohexane

: 169616-96-0
methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 81 percent / conc. sulfuric acid; nitric acid / CH₂Cl₂ / 2 h / 0 - 20 °C

2.1: 90 percent / hydrogen / Pd/C / ethanol / 3.5 h / 20 °C

3.1: 28 percent / n-BuLi / tetrahydrofuran; hexane / 3 h / 20 °C

4.1: n-BuLi / tetrahydrofuran; hexane / 12 h / 20 °C

4.2: 71 percent / tetrahydrofuran; hexane / 0 - 20 °C

With n-butyllithium; sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; 1.1: Nitration / 2.1: Reduction / 3.1: Methylation / 4.1: dithiocarboxylation / 4.2: Methylation;
DOI:10.1246/bcsj.72.2523

Reference yield:

: 173607-77-7
1-nitro-4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]benzene

: 169616-96-0
methyl N-methyl-N-{4-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]phenyl}dithiocarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / hydrogen / Pd/C / ethanol / 3.5 h / 20 °C

2.1: 28 percent / n-BuLi / tetrahydrofuran; hexane / 3 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 12 h / 20 °C

3.2: 71 percent / tetrahydrofuran; hexane / 0 - 20 °C

With n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; 1.1: Reduction / 2.1: Methylation / 3.1: dithiocarboxylation / 3.2: Methylation;
DOI:10.1246/bcsj.72.2523