2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

Base Information

Chemical Name:2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide
CAS No.:1585244-71-8
Molecular Formula:C₁₇H₁₉N₃O₃S
Molecular Weight:345.422
Hs Code.:

Synonyms:2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

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Chemical Property of 2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

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Technology Process of 2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

There total 4 articles about 2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1585244-95-6
C₁₆H₁₇N₃O₃S*C₂HF₃O₂

: 1585244-71-8
2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In methanol; water; at 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2014.02.028

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 1585244-71-8
2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfur; morpholine / ethanol / 12 h / 20 °C

2: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

3: dichloromethane / 2 h / 20 °C / Inert atmosphere

4: sodium tris(acetoxy)borohydride; acetic acid / methanol; water / 1 h / 20 °C

With morpholine; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; sulfur; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; ethanol; dichloromethane; water; 1: |Gewald Aminoheterocycles Synthesis;
DOI:10.1016/j.ejmech.2014.02.028

Reference yield:

: 1001020-08-1
tert-butyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate

: 1585244-71-8
2-(2-methoxybenzamido)-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

2: dichloromethane / 2 h / 20 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride; acetic acid / methanol; water / 1 h / 20 °C

With sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2014.02.028