1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

Base Information

Chemical Name:1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane
CAS No.:1360457-09-5
Molecular Formula:C₁₈H₃₄FN₃Si₂
Molecular Weight:367.657
Hs Code.:

Synonyms:1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

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Chemical Property of 1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

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Technology Process of 1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

There total 2 articles about 1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1360457-04-0
1,3-di-tert-butyl-2,2-difluoro-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

: lithium 3,5-dimethylphenylamide

: 1360457-09-5
1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

Guidance literature:: In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;
DOI:10.1002/zaac.201100346

Reference yield:

: 17940-08-8
bis(tert-butylamino)dimethylsilane

: 1360457-09-5
1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / Inert atmosphere; Reflux

1.2: -20 °C / Inert atmosphere

2.1: tetrahydrofuran; hexane / 0 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/zaac.201100346

Reference yield: 83.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1360457-09-5
1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane

: C₄H₈O*C₁₈H₃₃FN₃Si₂^(1-)*Li⁽¹⁺⁾

Guidance literature:: 1,3-di-tert-butyl-2-fluoro-2-(3,5-dimethylanilino)-4,4-dimethyl-1,3-diaza-2,4-disilacyclobutane; With n-butyllithium; In hexane; at 20 ℃; Inert atmosphere;

tetrahydrofuran; In hexane;
DOI:10.1002/zaac.201100346