2-amino-2-(4-decylphenyl)propane-1,3-diol

Base Information

Chemical Name:2-amino-2-(4-decylphenyl)propane-1,3-diol
CAS No.:162361-15-1
Molecular Formula:C₁₉H₃₃NO₂
Molecular Weight:307.477
Hs Code.:

Synonyms:2-amino-2-(4-decylphenyl)propane-1,3-diol

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Chemical Property of 2-amino-2-(4-decylphenyl)propane-1,3-diol

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Technology Process of 2-amino-2-(4-decylphenyl)propane-1,3-diol

There total 5 articles about 2-amino-2-(4-decylphenyl)propane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-72-3
decylbenzene

: 162361-15-1
2-amino-2-(4-decylphenyl)propane-1,3-diol

Guidance literature:: Multi-step reaction with 6 steps

1: TiCl₄ / CH₂Cl₂ / 1 h / 20 °C

2: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

3: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

4: 47 percent / AgNO₂ / diethyl ether / 4 h / 0 °C

5: 55 percent / aq. NaOH / ethanol; dioxane / 21 h / 20 - 50 °C

6: H₂ / Raney Ni / ethanol / 16 h / 20 °C / 15201 Torr

With sodium hydroxide; sodium tetrahydroborate; silver(I) nitrite; hydrogen; titanium tetrachloride; nickel; In 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; isopropyl alcohol; toluene; 1: Formylation / 2: Reduction / 3: Bromination / 4: Nitration / 5: hydroxymethylation / 6: Reduction;
DOI:10.1021/jm000173z

Reference yield:

: 70972-99-5
4-(n-decyl)benzaldehyde

: 162361-15-1
2-amino-2-(4-decylphenyl)propane-1,3-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

2: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

3: 47 percent / AgNO₂ / diethyl ether / 4 h / 0 °C

4: 55 percent / aq. NaOH / ethanol; dioxane / 21 h / 20 - 50 °C

5: H₂ / Raney Ni / ethanol / 16 h / 20 °C / 15201 Torr

With sodium hydroxide; sodium tetrahydroborate; silver(I) nitrite; hydrogen; nickel; In 1,4-dioxane; methanol; diethyl ether; ethanol; isopropyl alcohol; toluene; 1: Reduction / 2: Bromination / 3: Nitration / 4: hydroxymethylation / 5: Reduction;
DOI:10.1021/jm000173z

Reference yield:

: 162359-25-3
4-decylbenzyl bromide

: 162361-15-1
2-amino-2-(4-decylphenyl)propane-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / AgNO₂ / diethyl ether / 4 h / 0 °C

2: 55 percent / aq. NaOH / ethanol; dioxane / 21 h / 20 - 50 °C

3: H₂ / Raney Ni / ethanol / 16 h / 20 °C / 15201 Torr

With sodium hydroxide; silver(I) nitrite; hydrogen; nickel; In 1,4-dioxane; diethyl ether; ethanol; 1: Nitration / 2: hydroxymethylation / 3: Reduction;
DOI:10.1021/jm000173z