4-decylbenzyl bromide

Base Information

Chemical Name:4-decylbenzyl bromide
CAS No.:162359-25-3
Molecular Formula:C₁₇H₂₇Br
Molecular Weight:311.305
Hs Code.:

Synonyms:4-decylbenzyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-decylbenzyl bromide

Chemical Property:

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Technology Process of 4-decylbenzyl bromide

There total 3 articles about 4-decylbenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 7408-29-9
4-decylphenylmethanol

: 162359-25-3
4-decylbenzyl bromide

Guidance literature:: With 48percent aq. HBr; In toluene; at 90 ℃; for 24h;
DOI:10.1021/jm000173z

Reference yield:

: 104-72-3
decylbenzene

: 162359-25-3
4-decylbenzyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: TiCl₄ / CH₂Cl₂ / 1 h / 20 °C

2: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

3: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

With sodium tetrahydroborate; titanium tetrachloride; In methanol; dichloromethane; isopropyl alcohol; toluene; 1: Formylation / 2: Reduction / 3: Bromination;
DOI:10.1021/jm000173z

Reference yield:

: 70972-99-5
4-(n-decyl)benzaldehyde

: 162359-25-3
4-decylbenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

2: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

With sodium tetrahydroborate; In methanol; isopropyl alcohol; toluene; 1: Reduction / 2: Bromination;
DOI:10.1021/jm000173z