C₆₉H₆₈O₁₄

Base Information

Chemical Name:C₆₉H₆₈O₁₄
CAS No.:187031-92-1
Molecular Formula:C₆₉H₆₈O₁₄
Molecular Weight:1121.29
Hs Code.:

C<sub>69</sub>H<sub>68</sub>O<sub>14</sub>

Synonyms:C₆₉H₆₈O₁₄

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Chemical Property of C₆₉H₆₈O₁₄

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Technology Process of C₆₉H₆₈O₁₄

There total 8 articles about C₆₉H₆₈O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 187031-74-9
benzyl (benzyl 2,3-di-O-benzyl-β-D-galactopyranosid)uronate

: 187031-84-1
(2S,3R,4S,5R,6S)-4,5-Bis-benzyloxy-3-(4-methoxy-benzyloxy)-6-phenylsulfanyl-tetrahydro-pyran-2-carboxylic acid benzyl ester

: 187031-92-1
C₆₉H₆₈O₁₄

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In diethyl ether; dichloromethane; at -60 ℃; for 1.4h;
DOI:10.1016/S0040-4039(96)02308-8

Reference yield:

: 100-39-0
benzyl bromide

: 187031-92-1
C₆₉H₆₈O₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaHCO₃ sat., Aliquat 336 / CH₂Cl₂

2: 78 percent / NIS, CF₃SO₃H, 4 Angstroem molecular sieves / CH₂Cl₂; diethyl ether / 1.4 h / -60 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; Aliquat 336; sodium hydrogencarbonate; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(96)02308-8

Reference yield:

: 231623-55-5
phenyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranoside

: 187031-92-1
C₆₉H₆₈O₁₄

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine, DMAP

2: 1.) NaH

3: Dowex H⁺ / methanol

4: PDC / dimethylformamide

5: NaHCO₃ sat., Aliquat 336 / CH₂Cl₂

6: 78 percent / NIS, CF₃SO₃H, 4 Angstroem molecular sieves / CH₂Cl₂; diethyl ether / 1.4 h / -60 °C

With pyridine; dmap; N-iodo-succinimide; dipyridinium dichromate; trifluorormethanesulfonic acid; 4 A molecular sieve; Dowex H⁺; Aliquat 336; sodium hydride; sodium hydrogencarbonate; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(96)02308-8