7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid

Base Information

• Chemical Name: 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid
• CAS No.: 212501-36-5
• Molecular Formula: C₂₇H₂₄O₉
• Molecular Weight: 492.482

Synonyms:7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid

Chemical Property of 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid

Chemical Property:

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Technology Process of 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid

There total 1 articles about 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-benzyloxy-4-methoxy-2-(3,4,5-trimethoxybenzoyl)-benzoic acid (212500-89-5) + di-tert-butyl 2-bromomalonate (15960-79-9) → 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid (212501-36-5)

Guidance literature:

With hydrogenchloride; potassium carbonate; In 1,4-dioxane; N-methyl-acetamide; water; acetic acid; ethyl acetate;

Reference yield:

7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid (212501-36-5) → 7-benzyloxy-3hydroxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)-3,4-dihydroisocoumarin-3-carboxylic acid (212501-42-3)

Guidance literature:

With sodium hydroxide; In methanol;

Reference yield:

1-aminomorpholine (4319-49-7) + 7-benzyloxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)isocoumarin-3-carboxylic acid (212501-36-5) → 7-benzyloxy-3-carboxy-6-methoxy-2-morpholino-4-(3,4,5-trimethoxyphenyl)-1(2H)isoquinolinone

Guidance literature:

In 1,3-dimethyl-2-imidazolidinone; chloroform; water;

upstream raw materials:

5-benzyloxy-4-methoxy-2-(3,4,5-trimethoxybenzoyl)-benzoic acid

di-tert-butyl 2-bromomalonate

Downstream raw materials:

7-benzyloxy-3hydroxy-6-methoxy-4-(3,4,5-trimethoxyphenyl)-3,4-dihydroisocoumarin-3-carboxylic acid

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