(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

Base Information

Chemical Name:(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine
CAS No.:140440-42-2
Molecular Formula:C₂₄H₂₄Cl₂N₆O₂
Molecular Weight:499.4
Hs Code.:

Synonyms:(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

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Chemical Property of (+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

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Technology Process of (+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

There total 5 articles about (+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2028-74-2
p-chlorobenzenediazonium chloride

: 140440-41-1
(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-6-chloropyridimine

: 140440-42-2
(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

Guidance literature:: With sodium acetate; In methanol; water; for 6h; Ambient temperature;
DOI:10.1021/jm00088a026

Reference yield:

: 140440-35-3
(+/-)-5α-<(benzyloxy)methyl>-4β-(hydroxymethyl)cyclopent-2-en-1β-ylamine

: 140440-42-2
(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / triethylamine / ethanol / 40 h / 100 °C

2: 80 percent / AcONa / H₂O; methanol / 6 h / Ambient temperature

With sodium acetate; triethylamine; In methanol; ethanol; water;
DOI:10.1021/jm00088a026

Reference yield:

: 140440-34-2
ethyl (+/-)-N-<5α-<(benzyloxy)methyl>-4β-(hydroxymethyl)cyclopent-2-en-1β-yl>carbamate

: 140440-42-2
(+/-)-2-amino-4-<<5'α-<(benzyloxy)methyl>-4'β-(hydroxymethyl)cyclopent-2'-en-1'β-yl>amino>-5-<(4'-chlorophenyl)azo>-6-chloropyridimine

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / aq. KOH / methanol / 20 h / Heating

2: 80 percent / triethylamine / ethanol / 40 h / 100 °C

3: 80 percent / AcONa / H₂O; methanol / 6 h / Ambient temperature

With potassium hydroxide; sodium acetate; triethylamine; In methanol; ethanol; water;
DOI:10.1021/jm00088a026