N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester

Base Information

• Chemical Name: N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester
• CAS No.: 307924-47-6
• Molecular Formula: C₃₈H₃₂N₂O₄
• Molecular Weight: 580.683
• Mol file: 307924-47-6.mol

Synonyms:N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester

Chemical Property of N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester

There total 2 articles about N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Benzophenone imine (1013-88-3) + glycine 1,3-phenylenebis(methylene) ester bistrifluoracetate salt → N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester (307924-47-6)

Guidance literature:

In dichloromethane; for 24h;

DOI:10.1021/jo025928j

Reference yield:

Benzophenone imine (1013-88-3) + BOC-glycine (4530-20-5) + 1,3-dimethanol benzene (626-18-6) → N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester (307924-47-6)

Guidance literature:

BOC-glycine; 1,3-dimethanol benzene; With dmap; In tetrahydrofuran; dichloromethane; at 20 ℃; for 40h; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

Benzophenone imine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.201403046

Reference yield: 45.0%

fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) + N-(diphenylmethylene)glycine 1,3-phenylenebis(methylene) ester (307924-47-6) → C98H28N2O4

Guidance literature:

With carbon tetrabromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1002/ejoc.201403046

upstream raw materials:

Benzophenone imine

BOC-glycine

1,3-dimethanol benzene