N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

Base Information

Chemical Name:N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine
CAS No.:651048-16-7
Molecular Formula:C₃₆H₂₇N₉O₈
Molecular Weight:713.666
Hs Code.:

Synonyms:N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

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Technology Process of N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

There total 4 articles about N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 137730-90-6
N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

: 651048-16-7
N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 30 ℃; for 72h; under 11250900 Torr;
DOI:10.1055/s-2003-42434

Reference yield:

: 537-65-5
4,4'-diaminodiphenylamine

: 651048-16-7
N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98.6 percent / Et₃N / dimethylformamide / 72 h / 40 °C / 11250900 Torr

2: 68.1 percent / H₂ / Pd/C / methanol / 2068.59 Torr

3: 93.2 percent / Et₃N / dimethylformamide / 72 h / 30 °C / 11250900 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2003-42434

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 651048-16-7
N'',N'''-bis(2''',4'''-dinitrophenyl)-N,N'-bis(4''-aminophenyl)-4,4'-diaminodiphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98.6 percent / Et₃N / dimethylformamide / 72 h / 40 °C / 11250900 Torr

2: 68.1 percent / H₂ / Pd/C / methanol / 2068.59 Torr

3: 93.2 percent / Et₃N / dimethylformamide / 72 h / 30 °C / 11250900 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2003-42434