N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

Base Information

Chemical Name:N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester
CAS No.:76308-22-0
Molecular Formula:C₁₄H₂₆N₃O₂PS
Molecular Weight:331.419
Hs Code.:

Synonyms:N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

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Chemical Property of N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

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Technology Process of N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

There total 6 articles about N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 151-56-4,9002-98-6
ethyleneimine

: 76308-20-8
N-dichlorothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

: 76308-22-0
N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane;
DOI:10.1007/BF00951237

Reference yield:

: 104-03-0
4-nitrobenzeneacetic acid

: 76308-22-0
N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOH, H₂, 2.) HCl (conc.) / 1.) Raney Ni / 1.) H₂O, 130 deg C, 150 atm, 8 h

2: 11.4 g / pyridine / 5 h / Heating

3: 86 percent / HCl (gas) / 2 h / Heating

4: 80 percent / PSCl₃, Et₃N / diethyl ether

5: 72 percent / Et₃N / diethyl ether; CH₂Cl₂

With pyridine; hydrogenchloride; sodium hydroxide; hydrogen; triethylamine; trichlorophosphate; nickel; In diethyl ether; dichloromethane;
DOI:10.1007/BF00951237

Reference yield:

: 2952-01-4
(cis-4-amino-cyclohexyl)-acetic acid

: 76308-22-0
N-diethyleneimidothiophosphoryl-cis-4-aminocyclohexylacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 11.4 g / pyridine / 5 h / Heating

2: 86 percent / HCl (gas) / 2 h / Heating

3: 80 percent / PSCl₃, Et₃N / diethyl ether

4: 72 percent / Et₃N / diethyl ether; CH₂Cl₂

With pyridine; hydrogenchloride; triethylamine; trichlorophosphate; In diethyl ether; dichloromethane;
DOI:10.1007/BF00951237