3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Base Information

Chemical Name:3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether
CAS No.:1083084-79-0
Molecular Formula:C₂₇H₃₃NO₂
Molecular Weight:403.565
Hs Code.:

Synonyms:3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Suppliers and Price of 3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

There total 2 articles about 3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 474746-67-3
3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime

: 1083084-79-0
3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Guidance literature:: With sodium acetate; In water; acetonitrile; at 20 ℃; for 6h;
DOI:10.1016/j.steroids.2014.08.015

Reference yield:

: 118335-53-8
3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde

: 1083084-79-0
3-methoxy-14β-(prop-2-en-yl)-des-D-estra-1,3,5(10)-trien-13α-carbaldehyde oxime benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / acetonitrile; water / 1 h / 20 °C

2: sodium acetate / acetonitrile; water / 6 h / 20 °C

With hydroxylamine hydrochloride; sodium acetate; In water; acetonitrile;
DOI:10.1016/j.steroids.2014.08.015